EXTRACTION AND UTILIZATION OF PHENOLIC ANTIOXIDANTS FROM WILD AONLA (Emblica officinalis Gaertn.) FRUITS

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Date
2022-02
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UHF,NAUNI
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ABSTRACT The present studies entitled, “Extraction and utilization of phenolic antioxidants from wild aonla (Emblica officinalis Gaertn) fruits” were conducted during 2018-2020 in the department of Food Science and Technology, Dr Yashwant Singh Parmar University of Horticulture and Forestry, Nauni, Solan (HP). The aim of the study was to extract the phenolic antioxidants from wild fruits of aonla and utilized it for the development of antioxidant rich food products. Wild aonla (Emblica officinalis) fruit is known for its functional, therapeutical and medicinal properties. In this study, whole fruit from Sabathu location was selected on the basis of composition of maximum antioxidants as compared to other fruit parts. Whole fruit could be dried and converted into powder form (425 microns particle size) after drying under mechanical cabinet drier at 50±1 ºC. The dried aonla fruit powder contained total phenols (1522.18 mg/100 g), total flavonoids (435.44 mg/ 100 g), total tannins (8.81 mg/100 g), DPPH antioxidant activity (89.56 %), FRAP (55.67 μM Fe2+/100 g), ABTS+ scavenging activity (2.52 mg/100 g) and metal chelating activity (50.31 %). Among all, ultrasound assisted extraction method with 1:20 (powder: 70 % ethanol) ratio at 50±1 ºC sonicated for 15 minutes was selected on the basis of highest antioxidant activity for the extraction of phenolic antioxidants. The liquid phenolic extract could further be dried successfully under vacuum rotary evaporator at 50 ºC and preserved in glass vials. FT-IR as well as HPLC studies showed the appreciable amount of various components of antioxidants which include phenolic compounds like gallic acid, flavonoids, hydrolysable tannins, hamamelitannis, ethyl gallate, catechin gallate and rutin trihydrate. Antimicrobial studies have shown that phenolic compound have the capacity to check the activity of two popular bacteria Staphylococcus aureus and Escherichia coli. The phenolic extract of aonla was successfully encapsulated with maltodextrin (1:3) in freeze-drier at - 70 ºC and retained its quality for 4 months in ambered coloured glass vials under ambient (19-21ºC) and refrigerated (4-7 ºC) conditions, however, the quality was retained better under refrigerated temperature conditions as compared to ambient. The microencapsulated phenolic extract powder could further be utilized for the enrichment of food products like biscuit and mango drink. Both the products could be enriched successfully with microencapsulated phenolic extract powder at 2 (mango drink) and 3 per cent (biscuits) concentrations. Enriched biscuit could be stored for a period of 90 days in polyethylene pouch and drink for six months in PET bottles under ambient (19-21ºC) and refrigerated (4-7 ºC) storage conditions. However, minimum changes in the quality of both the products were observed under refrigerated storage conditions. Hence, wild aonla fruit can effectively be utilized for the extraction of phenolic antioxidants on commercial scale as well as for the development of antioxidant enriched products like biscuits and drinks. The cost of the products enriched with phenolic antioxidants was comparatively higher than the cost of the normal products in the market as higher cost can be paid by the consumer for additional health benefits of antioxidant enriched products
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